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TDSLab Series Thermal Desorption Spectrometers

TDSLab Series with shadows
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The TDSLab Series combines ultra-high-vacuum thermal desorption spectroscopy with quadrupole mass spectrometry for controlled studies of gases released from metals and advanced materials. Three configurations address sensitive hydrogen measurements in steel, high-mass species from semiconductor and photovoltaic materials, and hydrogen-isotope research.

UHV thermal desorption analysis for metals and advanced materials

TDSLab provides an integrated UHV workstation for temperature-programmed desorption and thermal desorption spectroscopy. Samples can be heated to 1,000 °C under PID control while the mass spectrometer records evolved species against temperature. A water-cooled shroud and mass-filter shroud help reduce background signals, and TPDsoft supports temperature-ramp control and synchronised data acquisition.

Choose TDSLab-6 for quantitative hydrogen desorption analysis in steel and other metals, with a detection capability of 0.01 ppm hydrogen in steel. The resulting hydrogen-desorption data support hydrogen embrittlement research by characterising hydrogen behaviour in steels and other advanced materials.

TDSLab-9 extends the mass range for photovoltaic and semiconductor research, while TDSLab-20 is configured for demanding fusion and isotope applications. These options allow laboratories to match sensitivity, mass range and sample configuration to the material under investigation.

Key features of the TDSLab thermal desorption mass spectrometer

• 1,000 °C sample stage with PID control module for precise temperature management
• High-precision triple-filter quadrupole mass spectrometer with a digital pulse-ion-counting detector for detailed gas analysis
• Multiport UHV chamber for complex experimental setups
• Water-cooled heater shroud to minimise outgassing and speed up cooling
• Linear sample-transfer mechanism and loadlock with a gate valve and viewports for operational flexibility
• Z-drive for optimal sample and detector positioning
• Mass-filter shroud to increase sensitivity and reduce background interference
• TPDsoft control and analysis software for experiment management and data analysis
• Bakeout jacket rated to 150 °C to reduce downtime between experiments

Related Products

Further Reading

Hiden’s TPDsoft thermal analysis PC software included with the Workstation provides automatic control of sample temperature integrated with analyser control. TPD analysis routines (e.g. peak integration/deconvolution etc) are also included in this package.
Application note AN-10012.2: Analysis of Hydrogen Isotopes in Metals by TPD/TDS

Application note AN-10035.1: Analysis of Coated Silicon Surfaces by TPD/TDS

Isothermal Desorption Spectroscopy (ITDS) | Imperial College London
Research using the Hiden TPD Workstation for Isothermal Desorption Spectroscopy (ITDS).

MRF Tritium Capability | NNUF
Research using the Hiden TPD Workstation for Thermal Desorption Spectroscopy (TDS).

Keszler Research Group | Oregon State University
Research is directed to the synthesis and study of inorganic molecules and materials that will enable next-generation electronic and energy devices

National Science Foundation
Sustainable chemistry center works to transform electronics manufacturing — Science Nation